2-甲氧基-4-硝基乙酰苯胺合成路线 (共 21 条)
参考文献
Ingold; Ingold
Journal of the Chemical Society, 1926 , p. 1319
参考文献
Ingold; Ingold
Journal of the Chemical Society, 1926 , p. 1319
反应条件
1: iron; aqueous acetic acid 2: aqueous sulfuric acid; sodium nitrite / Erhitzen der Reaktionsloesung mit Kupfer(I)-bromid View Scheme
参考文献
Hanford; Adams
Journal of the American Chemical Society, 1935 , vol. 57, p. 1592,1594
反应条件
1: iron; aqueous acetic acid 2: aqueous sulfuric acid; sodium nitrite / Erhitzen der Reaktionsloesung mit Kupfer(I)-bromid 3: Diazotization View Scheme
参考文献
Hanford; Adams
Journal of the American Chemical Society, 1935 , vol. 57, p. 1592,1594
参考文献
Fourneau; Trefouel; Benoit
Ann.Inst.Pasteur, 1930 , vol. 44, p. 719,748
反应条件
1: H2 / Raney nickel / methanol / 22.5 h / 2585.7 Torr 2: pyridine / CH2Cl2 / 25 °C 3: 82 percent / conc. HCl / ethanol; H2O / reflux, 5 h; 25 deg C, overnight View Scheme
参考文献
Brennan; Colbry; Leeds; Leja; Priebe; Reily; Showalter; Uhlendorf; Atwell; Denny
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 5 p. 1469 - 1476
反应条件
Bi(NO3)3·5H2O in dichloromethane
T=23°C; regioselective reaction;
参考文献
Lu, Yang; Li, Yaming; Zhang, Rong; Jin, Kun; Duan, Chunying
Tetrahedron, 2013 , vol. 69, # 45 p. 9422 - 9427
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
Ambient temperature;
参考文献
Pearson, Anthony J.; Park, Jewn G.; Zhu, Ping Y.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3583 - 3589
参考文献
Freyss
Chem. Zentralbl., 1901 , vol. 72, # I p. 738
Full Text Show Details
Fabr.de Thann et Mulhouse
Patent: DE98637 ;
Full Text Show Details
Meldola; Eyre
Chem. News J. Ind. Sci., 1901 , vol. 83, p. 1076,285
参考文献
Sundberg, Richard J.; Baxter, Ellen W.
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2687 - 2690