(3,4-二甲氧苯基)乙腈合成路线 （共 124 条）
反应条件
ethyl phosphorodichloridate; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=20°C; 2 h;
参考文献
Kuo, Chun-Wei; Zhu, Jia-Liang; Wu, Jen-Dar; Chu, Cheng-Ming; Yao, Ching-Fa; Shia, Kak-Shan
Chemical Communications, 2007 , # 3 p. 301 - 303
反应条件
Spirolt;cyclohexan-1,3'-oxaziridingt; in toluene T=20 - 25°C; 4 h;
参考文献
Andreae, Siegfried; Schmitz, Ernst
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 1008 - 1014
反应条件
iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=65°C; 3 h;
参考文献
Chiampanichayakul, Supanimit; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Kuhakarn, Chutima
Synthesis, 2008 , # 13 p. 2045 - 2048
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water in dimethyl sulfoxide T=130°C; Domino Suzuki coupling and fragmentation reaction; 16 h; Inert atmosphere;
参考文献
Velcicky, Juraj; Soicke, Arne; Steiner, Roland; Schmalz, Hans-Guenther
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6948 - 6951
反应条件
trimethylsilyl iodide; 1,1,1,3,3,3-hexamethyl-disilazane in chloroform T=56°C; 4 h;
参考文献
Jung, Michael E.; Long-Mei, Zeng
Tetrahedron Letters, 1983 , vol. 24, # 42 p. 4533 - 4534
反应条件
acetic acid; zinc T=100°C; 1 h;
参考文献
Tamura, Yasumitsu; Choi, Hong Dae; Mizutani, Masako; Ueda, Yuko; Ishibashi, Hiroyuki
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 10 p. 3574 - 3579
反应条件
1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C 3: acetonitrile / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 16 p. 2205 - 2208
反应条件
1: SOCl2 / dioxane / 20 °C 2: acetonitrile / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 16 p. 2205 - 2208
反应条件
in dimethyl sulfoxide 20 h;
参考文献
Mangla, V. K.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 9 p. 748 - 749
反应条件
diethylene glycol monoethyl ether; sodium amide in ethylene glycol dimethyl ether 1.) 45 deg C, 2 h, 2.) -10 deg C, 2 h, 3.) -45 deg C, 4.5 h;
参考文献
Synthetic Communications, , vol. 19, # 19 p. 3323 - 3330
