triethylamine in dichloromethane
T=-5°C; 0.666667 h;
参考文献
Vig, O. P.; Vig, R.; Dua, D. M.; Rani, Veena
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 274 - 275
1: 1.) NaH / 1.) THF, 20 deg C, 2.) 10 deg C, then room temp., 6 h, then 50-55 deg C, 4 h
2: 70 percent / lithium aluminium monoethoxy hydride / diethyl ether
3: 81 percent / NEt3 / CH2Cl2 / 0.67 h / -5 °C
View Scheme
参考文献
Vig, O. P.; Vig, R.; Dua, D. M.; Rani, Veena
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 274 - 275
Vig, O. P.; Vig, R.; Dua, D. M.; Rani, Veena
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 274 - 275
