3,6,9-三氧杂十一烷-1,11-二胺合成路线 （共 26 条）
反应条件
carbonylchlorohydridetris(triphenylphosphine) ruthenium(II); ammonia; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,1-dimethylpropan-1-ol T=140°C; 20 h; Inert atmosphereCooling;
参考文献
EVONIK DEGUSSA GmbH; Klasovsky, Florian; Tacke, Thomas; Pfeffer, Jan Christoph; Haas, Thomas; Beller, Matthias; Martin, Andreas; Deutsch, Jens; Koeckritz, Angela; Imm, Sebastian; Haberland, Juergen
Patent: US2013/331580 A1, 2013 ;
Location in patent: Paragraph 0063 ;
反应条件
hydrogen; palladium on barium sulfate in ethanol; water P=760 Torr; 30 h;
参考文献
Gunzenhauser; Biala; Strazewski
Nucleosides and Nucleotides, 1999 , vol. 18, # 6-7 p. 1223 - 1224
反应条件
hydrazine hydrate T=20°C;
参考文献
Lill, Andreas; Scholich, Klaus; Stark, Holger
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6682 - 6686
反应条件
hydrogenchloride; sodium chloride; citric acid in pyridine; ethanol
反应条件
1: 66 percent / dimethylformamide 2: 48 percent / 1) hydrazine hydrate, 2) 6N aq. HCl / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1301 - 1307
反应条件
ueber O,O'-Bis-<2-phthalimido-aethyl>-diaethylenglykol;
反应条件
1: acetonitrile / 12 h / Heating 2: HCl / ethanol / 2 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 79 - 84
反应条件
phosphoric acid; triphenylphosphine in diethyl ether; water 24 h; effect of dilution conditions; various reaction times; other reagent, solvent; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 63, # 5 p. 1727 - 1729
反应条件
1: 45 percent / DMAP / tetrahydrofuran / 3 h / 20 °C 2: 503 mg / TEA / dimethylformamide / 20 h 3: 52 percent / reaget K25 / 1.5 h / 20 °C View Scheme
参考文献
McReynolds, Katherine D.; Bhat, Abhijit; Conboy, John C.; Saavedra; Gervay-Hague, Jacquelyn
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 3 p. 625 - 637
反应条件
in methanol-d4 T=20°C; 12 h;
参考文献
Saggiomo, Vittorio; Luening, Ulrich
European Journal of Organic Chemistry, 2008 , # 25 p. 4329 - 4333
