1,8-二氨基-3,6-二氧杂辛烷合成路线 （共 65 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 10 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 18, p. 297 - 302
反应条件
hydrazine hydrate in ethanol 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 46, # 15 p. 3064 - 3070
参考文献
Journal of Organic Chemistry, , vol. 39, p. 1315 - 1316
反应条件
Pt on charcoal in tetrahydrofuran
反应条件
potassium hydroxide; ammonium hydroxide in 1,4-dioxane 1) 5 days 2) overnight;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 1077 - 1083
反应条件
1: 72 percent / dimethylformamide 2: 54 percent / 1) hydrazine hydrate, 2) 6N aq. HCl / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1301 - 1307
反应条件
1: 56 percent / PBr3, pyridine / 1) 20 - 22 deg C, 12 h, 2) 100 deg C, 1 h 2: 72 percent / dimethylformamide 3: 54 percent / 1) hydrazine hydrate, 2) 6N aq. HCl / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1124 - 1129
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1301 - 1307
反应条件
ammonia; nickel T=205°C;
参考文献
US2412209 , ;
US2357176 , ;
反应条件
1: 60 percent / methanol / 168 h / 25 °C / 750.06 Torr 2: 85 percent / lithium aluminium hydride (LAH) / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Dietrich,B. et al.
Tetrahedron, 1973 , vol. 29, p. 1629 - 1645
