in diethyl ether
dropwise addn. of soln. of Mg-compd. in diethyl ether to etheric soln. of Hg-compd. with stirring at -30°C, warming to -5°C, further stirring for 1.5 h; addn. of H2O (with ice cooling), sepn. of ether phase, drying over MgSO4, distillation, elem. anal.;
参考文献
Dimitrov, V.; Thiele, K.-H.; Radeglia, R.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1983 , vol. 503, p. 177 - 183
