5-溴-a,2-二氰基苯乙酸甲酯合成路线 (共 3 条)
反应条件
water in dimethyl sulfoxide T=115°C; 1 h;
参考文献
Frohn, Mike; Buerli, Roland W.; Riahi, Bobby; Hungate, Randall W.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 487 - 489
反应条件
1: 93 percent / H2O / dimethylsulfoxide / 1 h / 115 °C 2: 59 percent / HBr; dichloroacetic acid / 0 - 20 °C View Scheme
参考文献
Frohn, Mike; Buerli, Roland W.; Riahi, Bobby; Hungate, Randall W.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 487 - 489
反应条件
sodium hydride in dimethyl sulfoxide
T=90°C;
参考文献
Frohn, Mike; Buerli, Roland W.; Riahi, Bobby; Hungate, Randall W.
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 487 - 489