3,3-二甲基丙烯酸甲酯合成路线 (共 110 条)
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water
参考文献
Hendrickson, James B.; Boudreaux, Gerald J.; Palumbo, Paul S.
Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2358 - 2366
参考文献
Chattapadhyay, Tarun Kumar; Dureja, Prem
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 6 p. 2129 - 2133
反应条件
water in acetonitrile T=80°C; 12 h;
参考文献
Wiering, P.G.; Steinberg, H.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1663 - 1666
反应条件
4 A molecular sieve in dichloromethane 72 h; Irradiation; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5824 - 5831
反应条件
1: (carbomethoxymethyl)trimethylsilane With lithium hexamethyldisilazane in tetrahydrofuran T=0°C; 0.5 h; 2: acetone in tetrahydrofuran T=-78°C; 2 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 21 p. 7378 - 7388
反应条件
in tetrahydrofuran T=0°C;
参考文献
Rodriguez, Ana M.; Enriz, Ricardo D.; Santagata, Luis N.; Jauregui, Esteban A.; Pestchanker, Mauricio J.; Giordano, Oscar S.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 12 p. 1827 - 1834
反应条件
T=400°C; P=0.001 - 0.1 Torr;
参考文献
Aitken, R. Alan; Armstrong, Jill M.; Drysdale, Martin J.; Ross, Fiona C.; Ryan, Bruce M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1999 , # 5 p. 593 - 604
反应条件
1: 73 percent / Na2S / methanol 2: 1.) tosylhydrazine, 2.) aq. NaOH / 2.) pentane 3: 19 percent / methanol / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4804 - 4805
反应条件
1: 1.) tosylhydrazine, 2.) aq. NaOH / 2.) pentane 2: 19 percent / methanol / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4804 - 4805
反应条件
1: bromine / 0 °C 2: diethyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3216