4-乙酰氧基-N,N-二甲基色胺合成路线 （共 7 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 10 p. 2283 - 2287
反应条件
hydrogen; sodium acetate; palladium on activated charcoal in benzene P=3102.89 Torr; 4 h;
参考文献
Synthesis, , # 6 p. 935 - 938
反应条件
1: diethyl ether / 3 h / 5 - 10 °C 2: diethyl ether; CH2Cl2 / 6 h 3: 94.8 percent / LiAlH4 / tetrahydrofuran; dioxane / 1.) 4 h, 2.) reflux, 20 h 4: H2, AcONa / 10 percent Pd/C / benzene / 4 h / 3102.89 Torr View Scheme
参考文献
Synthesis, , # 6 p. 935 - 938
反应条件
1: 94.8 percent / LiAlH4 / tetrahydrofuran; dioxane / 1.) 4 h, 2.) reflux, 20 h 2: H2, AcONa / 10 percent Pd/C / benzene / 4 h / 3102.89 Torr View Scheme
参考文献
Synthesis, , # 6 p. 935 - 938
反应条件
1: tetrahydrofuran / 4 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 10 p. 2283 - 2287
反应条件
ethylene glycol dimethyl ether
参考文献
Helvetica Chimica Acta, , vol. 42, p. 2073,2098
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; P=760.051 Torr; 24 h;
参考文献
Furman, Svetlana; Nissim-Bardugo, Elinor; Zeeli, Shani; Weitman, Michal; Nudelman, Abraham; Finkin-Groner, Efrat; Moradov, Dorit; Shifrin, Helena; Schorer-Apelbaum, Donna; Weinstock, Marta
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 10 p. 2283 - 2287
