2,2-二氯-N,N-二乙基乙酰胺合成路线 （共 11 条）
反应条件
lithium diisopropyl amide Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Inoue, Rie; Shinokubo, Hiroshi; Oshima, Koichiro
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 910 - 911
反应条件
in dichloromethane
5 h; Heating;
参考文献
Concellon, Jose M.; Rodriguez-Solla, Humberto; Diaz, Pamela
Journal of Organic Chemistry, 2007 , vol. 72, # 21 p. 7974 - 7979
反应条件
1: With 1,4-diaza-bicyclo[2.2.2]octane; disulfur dichloride in chloroform
T=20°C; 72 h;
2: With formic acid in chloroform
1.5 h; Heating;
参考文献
Konstantinova; Berezin; Rakitin
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1178 - 1183
参考文献
Speziale,A.J.; Freeman,R.C.
Journal of the American Chemical Society, 1960 , vol. 82, p. 903 - 909
反应条件
phosphorous acid diethyl ester; triethylamine in benzene
12 h; Ambient temperature;
参考文献
Gertsyuk, M. N.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 4 p. 822 - 823
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 903 - 904
反应条件
in tetrachloromethane
T=-20°C; 0.333333 h;
参考文献
Voronina, T. A.; Fomina, N. V.; Suminov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 1059 - 1063
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 6 p. 1188 - 1192
参考文献
Dedek,V. et al.
Collection of Czechoslovak Chemical Communications, 1978 , vol. 43, p. 985 - 997
参考文献
Dedek,V. et al.
Collection of Czechoslovak Chemical Communications, 1978 , vol. 43, p. 2649 - 2655
反应条件
water; triethylamine in dimethyl sulfoxide
28 h; other solvent, other time.; Product distribution;
参考文献
Liska, Frantisek; Hampl, Frantisek; Dedek, Vaclav
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 3 p. 740 - 745
反应条件
in nitromethane
T=100°C; 1 h; Product distribution;
参考文献
Guseva, S. A.; Mirskova, A. N.; Levkovskaya, G. G.; Kalikhman, I. D.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 261 - 268
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 298 - 307
