二异丙基磷光体amidous二氯化物合成路线 （共 26 条）
反应条件
N-ethyl-N,N-diisopropylamine in hexane 2 h; Ambient temperature;
参考文献
Nurminen, Erkki J.; Mattinen, Jorma K.; Loennberg, Harri
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 7 p. 1621 - 1628
反应条件
triethylamine in diethyl ether
T=0°C; 2 h;
参考文献
Jennings, W. Brian; Tolley, Malcolm S.; Hargis, J. Howard; Worley, S. Davis; Chang, Lei
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1207 - 1212
反应条件
iodine; magnesium in tetrahydrofuran
Heating;
参考文献
King, R. Bruce; Sadanani, Narayan D.
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1719 - 1722
反应条件
in tetrahydrofuran
7 h; Inert atmosphereCooling with acetone-dry ice;
参考文献
Velian, Alexandra; Cummins, Christopher C.
Journal of the American Chemical Society, 2012 , vol. 134, # 34 p. 13978 - 13981
反应条件
1: 95 percent / KI, Al2Cl6 / CH2Cl2 / 10 h, -65 deg C then 3 h, -35 deg C then 5 h, -20 deg C then 10 h rt
2: diisopropylethylamine / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Farschtschi; Gorenstein
Tetrahedron Letters, 1988 , vol. 29, # 52 p. 6843 - 6846
反应条件
N-ethyl-N-isopropylamine
1.) CH2Cl2, -10 grad C, 30 min, 2.) CH2Cl2, 30 min; Yield given. Multistep reaction;
参考文献
Tanaka, Toshiki; Tamatsukuri, Sigeru; Ikehara, Morio
Tetrahedron Letters, 1986 , vol. 27, # 2 p. 199 - 202
