hydrazine hydrate in tetrahydrofuran; ethanol
T=60°C; 3 h;
参考文献
Dautel, Olivier J.; Robitzer, Mike; Lere-Porte, Jean-Pierre; Serein-Spirau, Francoise; Moreau, Joel J. E.
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16213 - 16223
1: 37 percent / Pd(OAc)2; CuI; DABCO / air / acetonitrile / 10 h / 20 °C
2: 70 percent / NH2NH2*H2O / ethanol; tetrahydrofuran / 3 h / 60 °C
View Scheme
参考文献
Dautel, Olivier J.; Robitzer, Mike; Lere-Porte, Jean-Pierre; Serein-Spirau, Francoise; Moreau, Joel J. E.
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16213 - 16223