2,6-二异丙基苯基氨基磺酸合成路线 (共 3 条)
反应条件
TEA in tetrahydrofuran
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 26 p. 5031 - 5034
反应条件
1: With chlorosulphonyl isocyanate in n-heptane
T=20°C; RefluxInert atmosphere;
2: With water in n-heptane
T=20°C; RefluxInert atmosphere;
参考文献
Asano, Shigehiro; Ban, Hitoshi; Tsuboya, Norie; Uno, Shinsaku; Kino, Kouichi; Ioriya, Katsuhisa; Kitano, Masafumi; Ueno, Yoshihide
Journal of Medicinal Chemistry, 2010 , vol. 53, # 8 p. 3284 - 3295
反应条件
water in dichloromethane
1 h; Heating;
参考文献
Hedayatullah, Mir; Hugueny, Jean Claude
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 167 - 172