反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 °C
1.2: tetrahydrofuran; hexane / -78 - 20 °C
1.3: 86 percent / aq. HCl / tetrahydrofuran; hexane / 1 h / 20 °C
2.1: tetrakis(triphenylphosphine)palladium(0) / 1,2-dimethoxy-ethane / 0.17 h / 20 °C
2.2: 88 percent / aq. Na2CO3 / 1,2-dimethoxy-ethane / 24 h / Heating
View Scheme
参考文献
Urselmann, Dominik; Antovic, Dragutin; Mueller, Thomas J. J.
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, art. no. 7, p. 1499 - 1503
