3-羟基-2,2,4-三甲基戊醛合成路线 (共 33 条)
反应条件
1-methyl-1H-imidazole; [Cu(MeCN)]4*CF3SO3; 4,4'-dimethoxy-2,2'-bipyridine; ABNO; oxygen in acetonitrile
T=20°C; 0.5 h;
参考文献
Steves, Janelle E.; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 42 p. 15742 - 15745
反应条件
titanium tetra-n-butoxide; potassium tert-butylate in tetrahydrofuran
T=0°C; self-aldol addition; 8 h;
参考文献
Han, Zhenfu; Yorimitsu, Hideki; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron Letters, 2000 , vol. 41, # 22 p. 4415 - 4418
反应条件
[Os(η(5)-C5,κ-N-Cp(N))(CH3CN)2]PF6 in THF-d8 (tetrahydrofuran-d8)
T=60°C; 3 h; Inert atmosphere;
参考文献
Batuecas, Maria; Esteruelas, Miguel A.; Garcia-Yebra, Cristina; Onate, Enrique
Organometallics, 2010 , vol. 29, # 9 p. 2166 - 2175
反应条件
titanium tetrachloride in dichloromethane
T=45°C;
参考文献
Kohler, Boris A. B.
Synthetic Communications, 1985 , vol. 15, p. 39 - 42
反应条件
in dimethyl sulfoxide
T=2°C; 16 h; enantioselective reaction;
参考文献
Rohr, Kerstin; Mahrwald, Rainer
Organic Letters, 2012 , vol. 14, # 8 p. 2180 - 2183
反应条件
Fe(2+)*C12H13N3*2CF3O3S(1-); dihydrogen peroxide in water; acetonitrile
T=20°C; 0.25 h; chemoselective reaction;
参考文献
Lenze, Matthew; Bauer, Eike B.
Chemical Communications, 2013 , vol. 49, # 52 p. 5889 - 5891
反应条件
bentonitic earth
Irradiation;
参考文献
Camarena; Cano; Delgado; Zuniga; Alvarez; Garcia
Tetrahedron Letters, 1993 , vol. 34, # 43 p. 6857 - 6858
反应条件
1,4-diaza-bicyclo[2.2.2]octane
Ambient temperature;
参考文献
Rafel, Sara; Leahy, James W.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1521 - 1522
参考文献
Fossek
Monatshefte fuer Chemie, 1883 , vol. 4, p. 671
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Brauchbar
Monatshefte fuer Chemie, 1896 , vol. 17, p. 643
参考文献
Alexander; Marvell
Journal of the American Chemical Society, 1950 , vol. 72, p. 1396
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Villani; Nord
Journal of the American Chemical Society, 1946 , vol. 68, p. 1674
Journal of the American Chemical Society, 1947 , vol. 69, p. 2606
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Grignard; Iliesco
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1930 , vol. 190, p. 557
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Saunders; Murray; Cleveland
Journal of the American Chemical Society, 1943 , vol. 65, p. 1715