2-氯-2-甲基丙烷-d9合成路线 （共 9 条）
反应条件
hypochlorite ion T=30.85°C; P=0.5 Torr; Kinetics;
参考文献
Villano, Stephanie M.; Kato, Shuji; Bierbaum, Veronica M.
Journal of the American Chemical Society, 2006 , vol. 128, # 3 p. 736 - 737
反应条件
magnesium; deuterium; platinum Multistep reaction;
参考文献
Fujisaki, Noboru; Ruf, Amanz; Gaeumann, Tino
Journal of the American Chemical Society, 1985 , vol. 107, # 6 p. 1605 - 1610
反应条件
aluminium trichloride T=0°C;
参考文献
Armstrong, Brian M.
Journal of the American Chemical Society, 1998 , vol. 120, # 24 p. 6007 - 6011
反应条件
aluminium trichloride in m-xylene T=20°C; Acylation; Friedels-Crafts acylation; 3 h;
参考文献
Riedel, Jens; Birner, Gerhard; Van Dorp, Corinne; Neumann, Hans-Guenter; Dekant, Wolfgang
Xenobiotica, 1999 , vol. 29, # 6 p. 573 - 582
反应条件
hydrogenchloride in water
参考文献
Zang, Yan; Kim, Jinheung; Dong, Yanhong; Wilkinson, Elizabeth C.; Appelman, Evan H.; Que Jr., Lawrence
Journal of the American Chemical Society, 1997 , vol. 119, # 18 p. 4197 - 4205
参考文献
Fujisaki, Noboru; Ruf, Amanz; Gaeumann, Tino
Journal of the American Chemical Society, 1985 , vol. 107, # 6 p. 1605 - 1610
反应条件
1: tert-butyl-d9 chloride With magnesium in diethyl ether
2 h; Heating;
2: carbon dioxide in diethyl ether
T=20°C; 0.5 h;
3: With sulfuric acid in diethyl ether
Further stages. Title compound not separated from byproducts.;
参考文献
Perrin, Charles L.; Dong, Yanmei
Journal of the American Chemical Society, 2007 , vol. 129, # 14 p. 4490 - 4497
反应条件
magnesium in tetrahydrofuran
参考文献
Fujisaki, Noboru; Ruf, Amanz; Gaeumann, Tino
Journal of the American Chemical Society, 1985 , vol. 107, # 6 p. 1605 - 1610
参考文献
Shull et al.
Journal of Chemical Physics, 1953 , vol. 21, p. 2024,2027
