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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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917612-13-6
合成路线
（共 10 条）
917611-89-3
→
反应条件
917612-13-6
反应条件
1: tetrahydrofuran / 12 h / 0 - 20 °C 2: TBAF / tetrahydrofuran / 6 h 3: Et3N / CH2Cl2 / 0 - 20 °C 4: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
37715-31-4
[5-(3,3-二甲基环氧乙烷-2-基)-3-甲基戊-2-烯基]乙酸酯
→
反应条件
917612-13-6
反应条件
1: HIO4*2H2O / diethyl ether; tetrahydrofuran / 0.5 h / 0 °C 2: NaBH4 / ethanol / 1 h / 0 °C 3: imidazole / dimethylformamide / 0 °C 4: K2CO3 / methanol / 1 h / 20 °C 5: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 6: tetrahydrofuran / 12 h / 0 - 20 °C 7: TBAF / tetrahydrofuran / 6 h 8: Et3N / CH2Cl2 / 0 - 20 °C 9: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
105-87-3
乙酸香叶酯
→
反应条件
917612-13-6
反应条件
1: 100 percent / mCPBA / CH2Cl2 / 2 h / -20 - 20 °C 2: HIO4*2H2O / diethyl ether; tetrahydrofuran / 0.5 h / 0 °C 3: NaBH4 / ethanol / 1 h / 0 °C 4: imidazole / dimethylformamide / 0 °C 5: K2CO3 / methanol / 1 h / 20 °C 6: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 7: tetrahydrofuran / 12 h / 0 - 20 °C 8: TBAF / tetrahydrofuran / 6 h 9: Et3N / CH2Cl2 / 0 - 20 °C 10: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
35334-60-2
→
反应条件
917612-13-6
反应条件
1: NaBH4 / ethanol / 1 h / 0 °C 2: imidazole / dimethylformamide / 0 °C 3: K2CO3 / methanol / 1 h / 20 °C 4: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 5: tetrahydrofuran / 12 h / 0 - 20 °C 6: TBAF / tetrahydrofuran / 6 h 7: Et3N / CH2Cl2 / 0 - 20 °C 8: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
100045-79-2
→
反应条件
917612-13-6
反应条件
1: imidazole / dimethylformamide / 0 °C 2: K2CO3 / methanol / 1 h / 20 °C 3: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 4: tetrahydrofuran / 12 h / 0 - 20 °C 5: TBAF / tetrahydrofuran / 6 h 6: Et3N / CH2Cl2 / 0 - 20 °C 7: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
162085-15-6
→
反应条件
917612-13-6
反应条件
1: Et3N / CH2Cl2 / 0 - 20 °C 2: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
187336-22-7
→
反应条件
917612-13-6
反应条件
1: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 2: tetrahydrofuran / 12 h / 0 - 20 °C 3: TBAF / tetrahydrofuran / 6 h 4: Et3N / CH2Cl2 / 0 - 20 °C 5: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
187336-21-6
→
反应条件
917612-13-6
反应条件
1: K2CO3 / methanol / 1 h / 20 °C 2: 90 percent / Et3N / hexane / 24 h / 0 - 20 °C 3: tetrahydrofuran / 12 h / 0 - 20 °C 4: TBAF / tetrahydrofuran / 6 h 5: Et3N / CH2Cl2 / 0 - 20 °C 6: 18-crown-6 / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
151-50-8
氰化钾
+
162085-16-7
→
反应条件
917612-13-6
反应条件
18-crown-6 ether in dichloromethane 6 h; Heating;
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
917612-13-6
+
917-54-4
甲基锂
→
反应条件
917612-30-7
反应条件
1: in diethyl ether T=-78 - 0°C; 2: With ammonium chloride in diethyl ether T=0°C; 0.166667 h;
参考文献
Uyanik, Muhammet; Ishihara, Kazuaki; Yamamoto, Hisashi
Organic Letters, 2006 , vol. 8, # 24 p. 5649 - 5652
