1-氨基-3-环戊烯盐酸盐合成路线 （共 9 条）
反应条件
1: Et3N / CH2Cl2 / 0.5 h / 0 °C 2: NaN3 / dimethylformamide / 16 h / 80 °C 3: 3.6 g / PPh3; water; aq. HCl / tetrahydrofuran; CH2Cl2 / 16 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 56, # 49 p. 9633 - 9640
反应条件
1: NaN3 / dimethylformamide / 16 h / 80 °C 2: 3.6 g / PPh3; water; aq. HCl / tetrahydrofuran; CH2Cl2 / 16 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 56, # 49 p. 9633 - 9640
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
O'Brien, Peter; Towers, Timothy D.; Voith, Matthias
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8175 - 8178
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C; Tosylation; 16 h;
参考文献
Barrett, Stephen; O'Brien, Peter; Steffens, H.Christian; Towers, Timothy D; Voith, Matthias
Tetrahedron, 2000 , vol. 56, # 49 p. 9633 - 9640
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
Barrett, Stephen; O'Brien, Peter; Steffens, H.Christian; Towers, Timothy D; Voith, Matthias
Tetrahedron, 2000 , vol. 56, # 49 p. 9633 - 9640
反应条件
pyridine; triethylamine in chloroform
参考文献
Patil, Sharadbala D.; Koga, Masakazu; Schneller, Stewart W.; Snoeck, Robert; Clercq, Erik De
Journal of Medicinal Chemistry, 1992 , vol. 35, # 12 p. 2191 - 2195
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
O'Brien, Peter; Towers, Timothy D.; Voith, Matthias
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8175 - 8178
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C;
参考文献
O'Brien, Peter; Towers, Timothy D.; Voith, Matthias
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8175 - 8178
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C; Acylation; 16 h;
参考文献
Barrett, Stephen; O'Brien, Peter; Steffens, H.Christian; Towers, Timothy D; Voith, Matthias
Tetrahedron, 2000 , vol. 56, # 49 p. 9633 - 9640
