反应条件
1: MeONa / methanol / 0 °C
2: 3.75 g / camphorsulfonic acid / acetonitrile / 20 °C
3: 67 percent / NIS; AgOTf / CH2Cl2 / 3 h / -70 - -50 °C
4: 75 percent / AcOH; zinc / 4 h / 20 °C
5: pyridine / 0.5 h / 20 °C
6: hydrogen / Pd(OH)2 on carbon / methanol; tetrahydrofuran
7: MeONa / methanol / 20 °C
View Scheme
参考文献
Fort, Sebastien; Kim, Hyo-Sun; Hindsgaul, Ole
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7146 - 7154
