lithium aluminium tetrahydride in tetrahydrofuran T=0°C;
参考文献
Greger, Jessica G.; Yoon-Miller, Sarah J. P.; Bechtold, Nathan R.; Flewelling, Scott A.; MacDonald, Jacob P.; Downey, Catherine R.; Cohen, Eric A.; Pelkey, Erin T.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8203 - 8214
1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2: dihydrogen peroxide; sodium hydrogencarbonate / methanol / 20 °C / Inert atmosphere
View Scheme
参考文献
Greger, Jessica G.; Yoon-Miller, Sarah J. P.; Bechtold, Nathan R.; Flewelling, Scott A.; MacDonald, Jacob P.; Downey, Catherine R.; Cohen, Eric A.; Pelkey, Erin T.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8203 - 8214