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91003-15-5
合成路线
(共 13 条)
91003-14-4
→
反应条件
91003-15-5
+
91003-16-6
反应条件
sodium hydroxide in methanol 3 h; Heating;
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-18-8
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反应条件
91003-15-5
反应条件
hydrogenchloride Ambient temperature;
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
6740-88-1
氯胺酮
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反应条件
91003-15-5
反应条件
1: 91 percent / anhydrous Na2CO3 / benzene / Heating 2: 1) lithium diisopropylamide 2) bromine / 1) THF, 1h, -78 deg C 2) 20 min, -78 deg C 3: 94.3 percent / dimethylformamide / 2 h / Heating 4: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-21-3
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反应条件
91003-15-5
+
91003-20-2
+
91003-27-9
反应条件
sodium carbonate; 3-chloro-benzenecarboperoxoic acid in hexane 1) 6h, room temperature 2) 1h, reflux;
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-19-9
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反应条件
91003-15-5
反应条件
1: 1) lithium diisopropylamide / 1) THF, 1h, -78 deg C 2) 10 min, -78 deg C 2: 2.5 g / m-chloroperoxybenzoic acid, anhydrous Na2CO3 / hexane / 1) 6h, room temperature 2) 1h, reflux View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-20-2
→
反应条件
91003-15-5
反应条件
1: 1) n-BuLi / 1) THF, 15 min, -78 deg C 2) -> room temperature 2: dimethylformamide / 5 h / steam bath 3: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-21-3
→
反应条件
91003-15-5
反应条件
1: 16 percent / m-chloroperoxybenzoic acid, anhydrous Na2CO3 / hexane / 1) 6h, room temperature 2) 1h, reflux 2: 1) n-BuLi / 1) THF, 15 min, -78 deg C 2) -> room temperature 3: dimethylformamide / 5 h / steam bath 4: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-12-2
→
反应条件
91003-15-5
反应条件
1: 1) lithium diisopropylamide 2) bromine / 1) THF, 1h, -78 deg C 2) 20 min, -78 deg C 2: 94.3 percent / dimethylformamide / 2 h / Heating 3: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-13-3
→
反应条件
91003-15-5
反应条件
1: 94.3 percent / dimethylformamide / 2 h / Heating 2: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
91003-23-5
→
反应条件
91003-15-5
反应条件
1: dimethylformamide / 5 h / steam bath 2: 41 percent / 1.0M NaOH / methanol / 3 h / Heating View Scheme
参考文献
Woolf, Thomas; Trevor, Anthony; Baillie, Thomas; Castagnoli, Neal
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3305 - 3310
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