7-二乙氨基-4-甲基香豆素合成路线 （共 55 条）
反应条件
oxygen in ethanol 15 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Kalmykova, E. A.; Kuznetsova, N. A.; Kaliya, O. L.; Tavrizova, M. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 4.2. p. 1003 - 1010,911 - 916
反应条件
oxygen Irradiation; Product distribution;
参考文献
Priyadarsini, K. Indira; Kunjappu, Joy T.; Moorthy, P. N.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1987 , vol. 26, # 11 p. 899 - 901
反应条件
sodium nitrite in acetic acid T=60 - 80°C; 8 h;
参考文献
Kirpichenok, M. A.; Gorozhankin, S. K.; Grandberg, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 7 p. 737 - 745
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 7 p. 888 - 897
反应条件
sodium acetate; acetone; copper dichloride
参考文献
Am. Cyanamid Co.
Patent: US2844594 , 1955 ;
反应条件
in acetonitrile
10 h; Irradiation; Yields of byproduct given;
参考文献
Kirpichenok, M. A.; Mel'nikova, L. M.; Denisov, L. K.; Grandberg, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 959 - 965
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1169 - 1175
反应条件
in acetonitrile
8 h; Irradiation;
参考文献
Kirpichenok, M. A.; Mel'nikova, L. M.; Denisov, L. K.; Grandberg, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 959 - 965
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1169 - 1175
反应条件
in ethanol
16 h; Irradiation; Further byproducts given;
参考文献
Kalmykova, E. A.; Kuznetsova, N.A.; Kaliya, O.L.; Zhigunova, G.A.; Sergeeva, N.D.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 7.2 p. 1658 - 1664,1361 - 1365
反应条件
1: 41 percent / SeO2 / xylene / 8 h / Heating
2: 88 percent / ethanol / 8 h / Ambient temperature
3: 80 percent / triethylamine / methanol / 5 h / Ambient temperature
View Scheme
参考文献
Ito, Keiichi; Maruyama, Junko
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3014 - 3023
反应条件
1: in para-xylene
24 h; Heating;
2: With sodium tetrahydroborate in ethanol
T=20°C; 4 h;
参考文献
Schoenleber, Ralph O; Bendig, Juergen; Hagen, Volker; Giese, Bernd
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 97 - 101
反应条件
selenium(IV) oxide; sodium borohydride in ethanol; para-xylene
参考文献
Cornell Research Foundation, Inc.
Patent: US2007/243519 A1, 2007 ;
