1,2,3,4-四氢异喹啉合成路线 (共 340 条)
反应条件
1: With sodium tetrahydroborate in ethanol 2: With sodium acetate; pyridinium chlorochromate 3: With potassium hydroxide in tetrahydrofuran; methanol Further stages.;
参考文献
Umetsu, Kazuteru; Asao, Naoki
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2722 - 2725
反应条件
L-Selectridereg; in tetrahydrofuran T=20°C; 72 h;
参考文献
Tetrahedron Letters, , vol. 39, # 49 p. 8933 - 8934
反应条件
aluminium trichloride in decalin T=180°C; 2 h;
参考文献
Synthetic Communications, , vol. 27, # 14 p. 2533 - 2538
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / Reflux 2.1: formic acid / 0.17 h / 0 °C 2.2: 24 h / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 42 p. 11787 - 11789
反应条件
1.1: ammonium acetate / acetic acid / 1.5 h / 20 °C / Reflux 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / Reflux 3.1: formic acid / 0.17 h / 0 °C 3.2: 24 h / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 42 p. 11787 - 11789
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid T=50°C; 1 h;
参考文献
Yokoyama, Akihiro; Ohwada, Tomohiko; Shudo, Koichi
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 611 - 617
反应条件
hydrogen; nickel T=200 - 205°C; P=12000.9 Torr; Mechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 8 p. 1321 - 1327
反应条件
hydrogenchloride in tert-butyl alcohol T=75°C; 10 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1977 - 1982
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in benzene T=80°C; 10 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1977 - 1982
反应条件
sodium hydroxide in tert-butyl alcohol T=75°C; 24 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1977 - 1982