1,2-二(溴甲基)苯 合成路线 （共 196 条）
参考文献
Bubb,W.A.; Sternhell,S.
反应条件
N-ethyl-N,N-diisopropylamine; C26H24BrOPPd; triphenylphosphine T=55°C; P=760.051 Torr; 2 h; Conversion of starting material;
参考文献
HERIOT-WATT UNIVERSITY
反应条件
sodium in toluene 24 h; Heating;
参考文献
Domiano, Paolo; Cozzini, Pietro; Claramunt, Rosa Maria; Lavandera, Jose Luis; Sanz, Dionisia; Elguero, Jose
参考文献
Dean; Berchet
参考文献
Baker et al.
反应条件
1: 67 percent / tetrahydrofuran; dimethylformamide / 96 h / Heating 2: tetrahydrofuran-d8 / 0.17 h / -95 °C / Irradiation 3: tetrahydrofuran-d8 / 0.03 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 13 p. 3564 - 3571
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反应条件
25676-64-6 1,3,4,7,8,10,11,13-八氢-6H-2,5,9,12-苯并四硫杂环十五烷
反应条件
caesium carbonate in N,N-dimethyl-formamide T=45 - 50°C;
参考文献
Buter, J.; Kellogg, Richard M.
反应条件
1: in N,N-dimethyl-formamide T=48°C; 48 h; 2: With PPA T=100 - 150°C; 18 h;
参考文献
Krapcho, A. Paul; Cadamuro, Sergio A.
反应条件
1: potassium carbonate / acetonitrile / 16 h / |Reflux; |Inert atmosphere 2: Pd0(tris(tert-butyl)phosphine)2 / cyclohexene; 1,4-dioxane / 24 h / 110 °C / |Inert atmosphere 3: 660 °C View Scheme
参考文献
Kreher, Richard P.; Kohl, Norbert
反应条件
1: 69 percent / Na2S*9H2O / Triethylhexadecylammonium-bromid / toluene; H2O / 24 h / Ambient temperature 2: 81 percent / 60percent H2O2, HOAc / 4 h / 0 °C 3: 40 percent / CH2Cl2 / 7 h / Ambient temperature 4: 77 percent / NEt3 / CH2Cl2 / 10 h / Ambient temperature View Scheme
参考文献
Zhen, Yonggang; Obata, Naoki; Matsuo, Yutaka; Nakamura, Eiichi
