N,N-二乙基-4-溴苯磺酰胺合成路线 （共 5 条）
反应条件
in dichloromethane T=0 - 25°C; sulfonylation; 12 h;
参考文献
Plobeck; Delorme; Wei; Yang; Zhou; Schwarz; Gawell; Gagnon; Pelcman; Schmidt; Yue; Walpole; Brown; Labare; Payza; St-Ogne; Kamassah; Morin; Projean; Ducharme; Roberts
Journal of Medicinal Chemistry, 2000 , vol. 43, # 21 p. 3878 - 3894
反应条件
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -30 °C 1.2: SO2 / tetrahydrofuran / 0.5 h / -40 °C 1.3: SO2Cl2 / tetrahydrofuran / -40 - 20 °C 2.1: 282 mg / tetrahydrofuran / 3 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 21 p. 8274 - 8276
反应条件
Cr3(OAc)7(OH)2; periodic acid in acetonitrile T=20°C; 20 h;
参考文献
Xu, Liang; Zhang, Suhong; Trudell, Mark L.
Synlett, 2004 , # 11 p. 1901 - 1904
反应条件
1: 89 percent / [Pd(PPh3)] / tetrahydrofuran / Heating 2: 85 percent / (i-Pr)2Mg; Ni(acac)2 / various solvent(s); diethyl ether / 8 h / 20 °C View Scheme
参考文献
Milburn, Robert R.; Snieckus, Victor
Angewandte Chemie - International Edition, 2004 , vol. 43, # 7 p. 888 - 891
反应条件
1: 89 percent / [Pd(PPh3)] / tetrahydrofuran / Heating 2: 72 percent / dppp; Ni(acac)2 / toluene; diethyl ether / Heating View Scheme
参考文献
Milburn, Robert R.; Snieckus, Victor
Angewandte Chemie - International Edition, 2004 , vol. 43, # 7 p. 888 - 891
