(4-甲基-2-噻唑)-苯胺合成路线 (共 10 条)
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=85°C; 15 h;
参考文献
Oehler, Elisabeth; Kang, Heun-Soo; Zbiral, Erich
Chemische Berichte, 1988 , vol. 121, p. 533 - 546
反应条件
1: 71 percent / ethanol / 108 h / Ambient temperature
2: 60 percent / CsF*H2O / dimethylformamide / 15 h / 85 °C
View Scheme
参考文献
Oehler, Elisabeth; Kang, Heun-Soo; Zbiral, Erich
Chemische Berichte, 1988 , vol. 121, p. 533 - 546
参考文献
Traumann
Justus Liebigs Annalen der Chemie, 1888 , vol. 249, p. 38
反应条件
in ethanol
20 h; Ambient temperature;
参考文献
Sharma,G.M. et al.
Tetrahedron, 1961 , vol. 15, p. 53 - 59
反应条件
hydrogenchloride
10 h; Heating;
参考文献
Murav'eva,K.M.; Shchukina,M.N.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2340 - 2343,2320 - 2323
反应条件
hydrogenchloride
9 h; Heating;
参考文献
Murav'eva,K.M.; Shchukina,M.N.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2340 - 2343,2320 - 2323
反应条件
in methanol
5 h; Heating;
参考文献
Schantl, Joachim G.; Lagoja, Irene M.
Synthetic Communications, 1998 , vol. 28, # 8 p. 1451 - 1462
参考文献
Hantzsch; Weber
Chemische Berichte, 1887 , vol. 20, p. 3130
反应条件
hydrogenchloride; ammonium hydroxide
1.) ethanol, 20 min, 80 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bramley, (Miss) Susan E.; Dupplin, Viscount; Goberdhan, Dhanesh G. C.; Meakins, G. Denis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 639 - 644
参考文献
Muraw'ewa; Schtschukina
Doklady Akademii Nauk SSSR, 1959 , vol. 126, p. 1274,1276
Doklady Chemistry, 124-129 <1959> 467, 469