2-甲基-5-吡咯烷-2-吡啶合成路线 （共 4 条）
反应条件
hydrogenchloride; sodium cyanoborohydride in methanol bromocresol green indicator;
参考文献
Seeman, Jeffrey I.; Secor, Henry V.; Chavdarian, Charles G.; Sanders, Edward B.; Bassfield, Ronald L.; Whidby, Jerry F.
Journal of Organic Chemistry, 1981 , vol. 46, # 15 p. 3040 - 3048
反应条件
1: conc.H2SO4 / 21 h / Heating 2: 1.) Diisopropylamine, n-BuLi/hexane, 2.) conc.HCl / 1.) ether, -70 deg C, 2.) water, reflux 3: 94 percent / sodium cyanoborohydride, 2N HCl / methanol / bromocresol green indicator View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 15 p. 3040 - 3048
反应条件
1: 1.) Diisopropylamine, n-BuLi/hexane, 2.) conc.HCl / 1.) ether, -70 deg C, 2.) water, reflux 2: 94 percent / sodium cyanoborohydride, 2N HCl / methanol / bromocresol green indicator View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 15 p. 3040 - 3048
反应条件
formic acid 12 h; Heating;
参考文献
Seeman, Jeffrey I.; Secor, Henry V.; Chavdarian, Charles G.; Sanders, Edward B.; Bassfield, Ronald L.; Whidby, Jerry F.
Journal of Organic Chemistry, 1981 , vol. 46, # 15 p. 3040 - 3048
