N-苄基-3-甲氧基苯胺合成路线 （共 20 条）
参考文献
Tosoh Corporation
Patent: US5929281 A1, 1999 ;
反应条件
sodium tetrahydroborate in methanol
T=20°C; 2 h;
参考文献
Garibotto, Francisco M.; Sortino, Maximiliano A.; Kouznetsov, Vladimir V.; Enriz, Ricardo D.; Zacchinoa, Susana A.
Arkivoc, 2011 , vol. 2011, # 7 p. 149 - 161
反应条件
triethylamine in dichloromethane
48 h; Heating;
参考文献
Pati, Hari; Weisbruch, Paul; Lemon, Adrienne; Lee, Moses
Synthetic Communications, 2004 , vol. 34, # 5 p. 933 - 940
反应条件
1: 71 percent / Et3N / CH2Cl2 / 18 h / Ambient temperature
2: 92 percent / LiAlH4 / tetrahydrofuran / 18 h / Heating
View Scheme
参考文献
Miah, Soyfur; Slawin, Alexandra M. Z.; Moody, Christopher J.; Sheehan, Scott M.; Marino Jr., Joseph P.; Semones, Mark A.; Padwa, Albert; Richards, Ian C.
Tetrahedron, 1996 , vol. 52, # 7 p. 2489 - 2514
反应条件
1: 71 percent / Et3N / CH2Cl2 / 18 h / Ambient temperature
2: 92 percent / LiAlH4 / tetrahydrofuran / 18 h / Heating
View Scheme
参考文献
Miah, Soyfur; Slawin, Alexandra M. Z.; Moody, Christopher J.; Sheehan, Scott M.; Marino Jr., Joseph P.; Semones, Mark A.; Padwa, Albert; Richards, Ian C.
Tetrahedron, 1996 , vol. 52, # 7 p. 2489 - 2514
反应条件
sulfuric acid; acetic acid; phenylacetylene
1) RT, 2) 70 deg C;
参考文献
Leardini, Rino; Nanni, Daniele; Tundo, Antonio; Zanardi, Giuseppe; Ruggieri, Fabrizio
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1842 - 1848
反应条件
1: ethanol / 5 h / Reflux
2: sodium tetrahydroborate / methanol / 2 h / 20 °C
View Scheme
参考文献
Garibotto, Francisco M.; Sortino, Maximiliano A.; Kouznetsov, Vladimir V.; Enriz, Ricardo D.; Zacchinoa, Susana A.
Arkivoc, 2011 , vol. 2011, # 7 p. 149 - 161
反应条件
1: anhydrous xylene / 2 h / |Reflux
2: copper(l) iodide; potassium tert-butylate; water / dimethyl sulfoxide / 8 h / 160 °C / |Inert atmosphere
View Scheme
参考文献
Zheng; Xu; Shi; Ren; Lu; Zhou
Asian Journal of Chemistry, 2013 , vol. 25, # 2 p. 1117 - 1122
反应条件
Pd0.3wt/TiO2
T=24.84°C; P=760.051 Torr; 12 h; IrradiationInert atmosphere; Mechanism; chemoselective reaction;
参考文献
Shiraishi, Yasuhiro; Fujiwara, Keisuke; Sugano, Yoshitsune; Ichikawa, Satoshi; Hirai, Takayuki
ACS Catalysis, 2013 , vol. 3, # 3 p. 312 - 320
参考文献
Hoerlein
Chemische Berichte, 1954 , vol. 87, p. 463,467, 470
