N-苄基-3-甲氧基苯胺合成路线 （共 20 条）
反应条件
sodium t-butanolate; palladium diacetate; CyPF-t-Bu in ethylene glycol dimethyl ether
T=100°C; 48 h;
参考文献
Shen, Qilong; Ogata, Tokutaro; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 20 p. 6586 - 6596
反应条件
biphenyl-2-yl-di-tert-butyl-phosphane; sodium t-butanolate; palladium dichloride in toluene
T=80°C; 23 h;
参考文献
Zhang, Xiao-Xiang; Harris, Michele C.; Sadighi, Joseph P.; Buchwald, Stephen L.
Canadian Journal of Chemistry, 2001 , vol. 79, # 11 p. 1799 - 1805
反应条件
CyPF-t-Bu; sodium t-butanolate; palladium diacetate in ethylene glycol dimethyl ether
T=80°C; 48 h;
参考文献
Shen, Qilong; Ogata, Tokutaro; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 20 p. 6586 - 6596
反应条件
1: With sodium tris(acetoxy)borohydride; acetic acid in dichloromethane
T=20°C; 16 h; Inert atmosphere;
2: With sodium hydroxide
参考文献
Arnott, Gareth; Brice, Heloise; Clayden, Jonathan; Blaney, Emma
Organic Letters, 2008 , vol. 10, # 14 p. 3089 - 3092
反应条件
potassium phosphate; copper monoiodide in ethylene glycol
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
1: m-methoxynitrobenzene With hydrogen; palladium on activated charcoal in ethanol
T=20°C; 2 h;
2: benzaldehyde in ethanol
T=20°C; 18 h;
3: With hydrogen; palladium on activated charcoal in ethanol
T=20°C; 0.25 h; Further stages.;
参考文献
Sydnes, Magne O.; Kuse, Masaki; Isobe, Minoru
Tetrahedron, 2008 , vol. 64, # 27 p. 6406 - 6414
反应条件
choline chloride urea
T=50°C; 1.5 h; chemoselective reaction;
参考文献
Singh, Balvant; Lobo, Hyacintha; Shankarling, Ganapati
Catalysis Letters, 2011 , vol. 141, # 1 p. 178 - 182
反应条件
cesium fluoride in acetonitrile
T=20°C; 5 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
18 h; Heating;
参考文献
Miah, Soyfur; Slawin, Alexandra M. Z.; Moody, Christopher J.; Sheehan, Scott M.; Marino Jr., Joseph P.; Semones, Mark A.; Padwa, Albert; Richards, Ian C.
Tetrahedron, 1996 , vol. 52, # 7 p. 2489 - 2514
反应条件
copper(l) iodide; potassium tert-butylate; water in dimethyl sulfoxide
T=160°C; 8 h; Inert atmosphere;
参考文献
Zheng; Xu; Shi; Ren; Lu; Zhou
Asian Journal of Chemistry, 2013 , vol. 25, # 2 p. 1117 - 1122
