反应条件
1: 86 percent / DIBALH / CH2Cl2 / 0.75 h / -10 °C
2: 1.) PBr3, 3.) PPTS
3: 99 percent / LiAlH4 / diethyl ether / 2 h / 0 °C
4: 23 percent / PPTS, H2O / acetone / 65 °C
View Scheme
参考文献
Eskola, Philip; Hirsch, Jerry A.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5732 - 5742
