3',5'-二甲氧基-4'-羟基-(2-羟基)苯乙酮合成路线 （共 9 条）
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Echeverri, Fernando; Quinones, Winston; Torres, Fernando; Duque, Mario; Archbold, Rosendo
Molecules, 2000 , vol. 5, # 12 p. 1287 - 1290
反应条件
1: methanol / 8 h / 20 °C
2: 60 percent / t-BuOK
3: 10 percent / 10 percent HCl / 5 h / Heating
4: 95 percent / H2 / Pd/C / methanol
View Scheme
参考文献
Echeverri, Fernando; Quinones, Winston; Torres, Fernando; Duque, Mario; Archbold, Rosendo
Molecules, 2000 , vol. 5, # 12 p. 1287 - 1290
反应条件
1: 68 percent / cupric bromide / CHCl3; ethyl acetate / 21 h / 20 °C
2: DBU / dioxane / 12 h / 0 - 20 °C
3: TFA / 4 h / 0 °C
4: H2O / UV-irradiation
View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: DBU / dioxane / 12 h / 0 - 20 °C
2: TFA / 4 h / 0 °C
3: H2O / UV-irradiation
View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
hydrogenchloride in ethanol
T=80°C; 1.5 h;
参考文献
Song; Shibuya; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 9 p. 2347 - 2350
反应条件
1: TFA / 4 h / 0 °C
2: H2O / UV-irradiation
View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: 98 percent / TFA / 4 h / 0 °C
2: H2O / UV-irradiation
View Scheme
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
反应条件
1: iodobenzene diacetate; KOH / methanol / 20 °C
2: 6 percent HCl / 1 h / 60 °C
View Scheme
参考文献
Luis, Javier G.; Andres, Lucia S.
Journal of Chemical Research - Part S, 1999 , # 3 p. 220 - 221
反应条件
water
Hydrolysis; reduction; UV-irradiation;
参考文献
Conrad II, Peter G.; Givens, Richard S.; Weber, Joerg F. W.; Kandler, Karl
Organic Letters, 2000 , vol. 2, # 11 p. 1545 - 1547
