(5E)-5-(2,3-二氯亚苄基)-2-疏基-1,3-噻唑-4(5H)-酮合成路线 (共 4 条)
反应条件
1: 85 percent / alkaline hydrolysis 2: 30 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 80 °C View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 85 percent / alkaline hydrolysis 2: 30 percent / NaOH / hexamethylphosphoric acid triamide / 5.5 h / 80 °C 3: Cu-quinoline View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
sodium acetate in acetic acid
6 h;
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 1.) NaNO2, hydrochloric acid, 2.) hydrated CuSO4, anhyd. NaSO3, NaOAc. 3.) hydrochloric acid
2: 70 percent / NaOAc / acetic acid / 6 h
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390