1-乙基-1H-苯并咪唑-2-磺酸合成路线 （共 7 条）
反应条件
ammonium formate T=150 - 160°C; Yield given. Yields of byproduct given;
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 2 p. 224
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 4 p. 266 - 267
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.; Makarov, S. P.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 12 p. 1348 - 1352
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 12 p. 1673 - 1677
反应条件
potassium hydroxide
T=50°C; 4 h;
参考文献
Divaeva; Kuzmenko; Morkovnik; Komissarov
Chemistry of Heterocyclic Compounds, 2006 , vol. 42, # 4 p. 463 - 468
反应条件
1: S-powder / 240 - 260 °C
2: NaOH, 30percent H2O2 / H2O
3: 86.3 percent / NaOH / aq. ethanol / 1 h
View Scheme
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.; Makarov, S. P.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 12 p. 1348 - 1352
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 12 p. 1673 - 1677
反应条件
1: S-powder / 240 - 260 °C
2: NaOH, 30percent H2O2 / H2O / 1) ice-cooling, 2) standing overnight
View Scheme
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.; Makarov, S. P.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 12 p. 1348 - 1352
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 12 p. 1673 - 1677
反应条件
1: NaOH, 30percent H2O2 / H2O
2: 86.3 percent / NaOH / aq. ethanol / 1 h
View Scheme
参考文献
Popov, I. I.; Boroshko, S. L.; Tertov, B. A.; Makarov, S. P.; Simonov, A. M.; Simkin, B. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 12 p. 1348 - 1352
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 12 p. 1673 - 1677
参考文献
Anisimova, V. A.; Levchenko, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 1 p. 48 - 52
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 1 p. 59 - 63
