1: SOCl2 / benzene / 48 h / 20 °C
2: 22.9 g / 18-crown-6 / acetonitrile / 48 h / 20 °C
3: 33 percent / Raney nickel / methanol / 48 h / 20 °C
4: 99 percent / CF3CO2H / 0.17 h / 20 °C
5: Heating
View Scheme
参考文献
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
1: 22.9 g / 18-crown-6 / acetonitrile / 48 h / 20 °C
2: 33 percent / Raney nickel / methanol / 48 h / 20 °C
3: 99 percent / CF3CO2H / 0.17 h / 20 °C
4: Heating
View Scheme
参考文献
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
1: 33 percent / Raney nickel / methanol / 48 h / 20 °C
2: 99 percent / CF3CO2H / 0.17 h / 20 °C
3: Heating
View Scheme
参考文献
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
1: 99 percent / CF3CO2H / 0.17 h / 20 °C
2: Heating
View Scheme
参考文献
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
