2-(6-甲氧基-3-吡啶)丙二酸二乙酯合成路线 (共 3 条)
反应条件
sodium hydroxide; water in tetrahydrofuran 2 h; Heating;
参考文献
Zhang, Xuqing; Sui, Zhihua
Synthesis, 2006 , # 15 p. 2568 - 2572
反应条件
sodium hydride; copper(I) bromide in 1,4-dioxane
T=100°C;
参考文献
Zhang, Xuqing; Sui, Zhihua
Synthesis, 2006 , # 15 p. 2568 - 2572
反应条件
Cu; caesium carbonate in dimethyl sulfoxide
T=70°C; Ullmann Condensation; 7 h; Inert atmosphere;
参考文献
Pai, Gita; Chattopadhyay, Asoke P.
Synthesis (Germany), 2013 , vol. 45, # 11 art. no. SS-2013-N0034-OP, p. 1475 - 1482