1: With magnesium in tetrahydrofuran T=20°C; 1 h; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; 49 h; 3: With water T=20°C; 1 h; Further stages.;
参考文献
Contreras; Parrot; Sippl; Rival; Wermuth
Journal of Medicinal Chemistry, 2001 , vol. 44, # 17 p. 2707 - 2718
1: With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; Inert atmosphere; 2: With tri-isopropoxy-borane in tetrahydrofuran; pentane T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran; water; pentane 0.5 h;
参考文献
Zehm, Daniel; Fudickar, Werner; Hans, Melanie; Schilde, Uwe; Kelling, Alexandra; Linker, Torsten
Chemistry - A European Journal, 2008 , vol. 14, # 36 p. 11429 - 11441
in water
thallic chloride in H2O was refluxed with o-ethylphenylboronic acid, giving a product after 1 min; the product was filtered off, washed with cold water, recrystd. from MeOH, and dried; elem. anal.;
参考文献
Cheesman, Bruce Victor; White, Raymond Frederick Martin
Canadian Journal of Chemistry, 1984 , vol. 62, p. 521 - 525
