反应条件
1: diazomethyl-trimethyl-silane With n-butyllithium in diethyl ether; hexane
T=0°C; 1 h;
2: 4,4'-bis-(N,N-dimethylamino)-benzophenone in tetrahydrofuran; diethyl ether; hexane
T=0 - 20°C; 2 h;
参考文献
Finke, Aaron D.; Dumele, Oliver; Zalibera, Michal; Confortin, Daria; Cias, Pawel; Jayamurugan, Govindasamy; Gisselbrecht, Jean-Paul; Boudon, Corinne; Schweizer, W. Bernd; Gescheidt, Georg; Diederich, Francois
Journal of the American Chemical Society, 2012 , vol. 134, # 43 p. 18139 - 18146