(alphaS)-rel-alpha-[(1R)-1-(甲基氨基)乙基]-苯甲醇合成路线 （共 56 条）
参考文献
Shono,Tatsuya; Matsumura, Yoshihiro; Kanazawa, Takenobu
Tetrahedron Letters, 1983 , vol. 24, # 42 p. 4577 - 4580
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 12 h; Heating;
参考文献
Heathcock, Clayton H.; Buse, Charles T.; Kleschick, William A.; Pirrung, Michael C.; Sohn, John E.; Lampe, John
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1066 - 1081
反应条件
1: 47 percent / 1) LDA 2: 96 percent / Heating 3: 79 percent / H2 / PtO2 / acetic acid / 0.5 h 4: 95 percent / KOH View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 42 p. 4577 - 4580
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 35, p. 620
Archiv der Pharmazie (Weinheim, Germany), , vol. 253, p. 89
Chem. Zentralbl., , vol. 98, # I p. 2538
反应条件
platinum(IV) oxide; ethanol
参考文献
Journal of the American Chemical Society, , vol. 51, p. 282
反应条件
1: 96 percent / Heating 2: 79 percent / H2 / PtO2 / acetic acid / 0.5 h 3: 95 percent / KOH View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 42 p. 4577 - 4580
反应条件
1: 79 percent / H2 / PtO2 / acetic acid / 0.5 h 2: 95 percent / KOH View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 42 p. 4577 - 4580
反应条件
potassium hydroxide; nickel monoaluminide in methanol T=25°C; Reduction; denitrosation; 24 h; Title compound not separated from byproducts;
参考文献
Organic Preparations and Procedures International, , vol. 23, # 2 p. 139 - 146
反应条件
methanol; platinum P=36775.4 Torr; Hydrogenation;
参考文献
Memoirs of the Institute of Scientific and Industrial Research, Osaka University, , vol. 6, p. 96,98
反应条件
1.1: CrO3; aq. H2SO4 / 2 h / 40 °C 1.2: 62 percent / NaNO2 / CH2Cl2 / 20 °C 2.1: 84 percent / NaOH; Na2CO3 / dimethylformamide / 1.25 h / 25 °C 3.1: aluminum-copper alloy; aq. KOH / methanol / 24 h / 25 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 23, # 2 p. 139 - 146
