2-羟基-4,6-二甲氧基苯乙酮合成路线 （共 113 条）
反应条件
potassium carbonate in acetone 3 h; Reflux;
参考文献
Seo, Young Ho; Oh, Yong Jin
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 12 p. 3782 - 3786
反应条件
1: 3,5-dimethoxy-phenol With boron trichloride in dichloromethane T=-10°C; Friedel-Crafts Acylation; 0.0833333 h; Inert atmosphere; 2: acetyl chloride in dichloromethane Friedel-Crafts Acylation; 3 h; RefluxInert atmosphere;
参考文献
Bazin, Marc-Antoine; Bodero, Lizeth; Tomasoni, Christophe; Rousseau, Benedicte; Roussakis, Christos; Marchand, Pascal
European Journal of Medicinal Chemistry, 2013 , vol. 69, p. 823 - 832
反应条件
boron tribromide in dichloromethane T=20°C; 0.333333 h;
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
potassium carbonate; dimethyl sulfate in acetone
参考文献
Tsumura and Co.
Patent: US5106871 A1, 1992 ;
反应条件
hydrogenchloride; aluminium trichloride; water 1.) Et2O, reflux, 1 h then r.t., overnight; Yield given. Multistep reaction;
参考文献
Phytochemistry (Elsevier), , vol. 28, # 11 p. 3193 - 3196
反应条件
potassium carbonate in acetone 12.5 h; Heating / reflux;
参考文献
US2006/63801 A1, ;
Page/Page column 5 ;
反应条件
dimethyl sulfate in chloroform
反应条件
potassium carbonate in ethanol T=80°C; 3 h;
参考文献
Wang, Jin; Zhou, Rong-Guang; Wu, Ting; Yang, Tao; Qin, Qi-Xue; Li, Li; Yang, Bo; Yang, Jian
Journal of Chemical Research, 2012 , vol. 36, # 3 p. 121 - 122
反应条件
potassium carbonate in acetone Heating;
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Chandler, I. Michael; McIntyre, C. Rupert; Simpson, Thomas J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2271 - 2284
