1: methyl iodide With Sn[N(SiMe3)2]2 in tetrahydrofuran T=20°C; 0.0833333 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3: monoiodonaphthalene With tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane 0.0333333 h; Heating; Further stages.;
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in ethanol; N,N-dimethyl-formamide T=80°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 117, # 23 p. 6345 - 6354