N-甲基-N-苯基苯磺酰胺合成路线 （共 20 条）
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=-78°C; 2 h; other arenesulfonyl derivatives, other temperatures; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 61, # 4 p. 1392 - 1398
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium; water; lithium n-butoxide 1.) THF, -78 deg C, 2 h, 2.) THF, 25 deg C, benzophenone presence or absence; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Eisch, John J.; Qian, Yun; Chiu, Chingchen S.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1392 - 1398
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium; water 1.) THF, -78 deg C, 2 h, 2.) THF, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Eisch, John J.; Qian, Yun; Chiu, Chingchen S.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1392 - 1398
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium; lithium n-butoxide in tetrahydrofuran T=-78°C; 2 h;
参考文献
Eisch, John J.; Qian, Yun; Chiu, Chingchen S.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1392 - 1398
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile 3 h; Heating;
参考文献
Sabitha, Gowravaram; Subba Reddy; Abraham, Sunny; Yadav
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1569 - 1570
参考文献
Michler; Meyer,K.
Chemische Berichte, 1879 , vol. 12, p. 1792
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in N,N-dimethyl-formamide
T=100°C; 24 h;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
potassium phosphate; copper(l) iodide; N,N-dimethylaminoacetic acid in N,N-dimethyl-formamide
48 h; Heating;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran
T=-78°C; 3 h;
参考文献
Eisch, John J.; Qian, Yun; Chiu, Chingchen S.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1392 - 1398
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in m-xylene
Heating;
参考文献
Ryokawa, Atsushi; Togo, Hideo
Tetrahedron, 2001 , vol. 57, # 28 p. 5915 - 5921
