2,3,5,6-四氟苯甲胺合成路线 （共 4 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran; water
参考文献
Doyon, Jeffrey B.; Jain, Ahamindra
Organic Letters, 1999 , vol. 1, # 2 p. 183 - 185
反应条件
1: With sulfuric acid; hydrogen; palladium on activated carbon
T=70°C; 3.3 h;
2: With water
T=100°C; 1 h; Product distribution / selectivity;
参考文献
SHOWA DENKO K.K.
Patent: WO2006/137347 A2, 2006 ;
Location in patent: Page/Page column 20-21; 33 ;
反应条件
1: With sulfuric acid; hydrogen; 5 rhodium-on-charcoal
T=20 - 80°C; 5.5 - 8.3 h;
2: With water
T=100°C; 1 h; Product distribution / selectivity;
参考文献
SHOWA DENKO K.K.
Patent: WO2006/137347 A2, 2006 ;
Location in patent: Page/Page column 18-20; 21-24; 27-28; 30-31; 33-34 ;
反应条件
1: With sulfuric acid; hydrogen; 5 rhodium-on-charcoal
T=70°C; 4.2 - 7 h;
2: With water
T=100°C; 1 h; Product distribution / selectivity;
参考文献
SHOWA DENKO K.K.
Patent: WO2006/137347 A2, 2006 ;
Location in patent: Page/Page column 26-27; 28-29; 34 ;
