4'-(4-溴苯基)-α,α',α''-三吡啶合成路线 （共 14 条）
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in tetrahydrofuran; water T=85°C; Suzuki-Miyayra cross-coupling; 48 h; Sealed tube;
参考文献
Nie, Hai-Jing; Yao, Jiannian; Zhong, Yu-Wu
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4771 - 4775
反应条件
ammonia
T=175°C; P=114008 Torr; 48 h;
参考文献
Mutai, Toshiki; Cheon, Jin-Dong; Arita, Shinpei; Araki, Koji
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 7 p. 1045 - 1050
反应条件
1: 4′-(p-bromophenyl)-2,2′,6′,2′′-terpyridine With n-butyllithium
T=-78 - 20°C;
2: boric acid trimethyl ester T=-78 - 20°C;
参考文献
Fu, She Han; Higuchi, Masayoshi; Kurth, Dirk G.
Organic Letters, 2007 , vol. 9, # 4 p. 559 - 562
反应条件
1: 4′-(p-bromophenyl)-2,2′,6′,2′′-terpyridine With n-butyllithium
T=-78 - 20°C;
2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane T=-78 - 20°C;
参考文献
Fu, She Han; Higuchi, Masayoshi; Kurth, Dirk G.
Organic Letters, 2007 , vol. 9, # 4 p. 559 - 562
