triethylamine; 3-chloro-benzenecarboperoxoic acid in diethyl ether 2 h; Ambient temperature;
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
1: 69 percent / 1.) -23 deg C, 5.25 h, 2.) room temperature, 45 min
2: 75 percent / Raney nickel / ethanol / 20 h / 90 °C
3: 88 percent / HBF4*Et2O / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
1: 75 percent / Raney nickel / ethanol / 20 h / 90 °C
2: 88 percent / HBF4*Et2O / CH2Cl2 / 1 h / Ambient temperature
View Scheme
参考文献
Fleming, Ian; Henning, Rolf; Parker, David C.; Plaut, Howard E.; Sanderson, Philip E. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 317 - 338
