反应条件
1: triethylamine / CHCl3
2: POCl3 / 0.5 h / 100 - 110 °C
3: 96.3 percent / 2N NaOH / ethanol / 0.25 h / 90 deg C bath
4: SOCl2 / 1 h / Heating
5: NaBH4, 2N HCl / 1,2-dimethoxy-ethane / ice cooling 30 min, reflux 30 min
View Scheme
参考文献
Meguro; Tawada; Sugiyama; Fujita; Kawamatsu
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2840 - 2851
