N-Boc-2-氨基乙醛合成路线 （共 17 条）
反应条件
lithium aluminium tetrahydride T=0°C; 0.25 h;
参考文献
Falkiewicz; Wisniowski; Kolodziejczyk; Wisniewski
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 4-7 p. 1393 - 1397
反应条件
Dess-Martin periodane in dichloromethane T=0°C; 0.5 h; Inert atmosphere;
参考文献
Bendiabdellah, Yassine; Villanueva-Margalef, Isabel; Misale, Antonio; Nahar, Kazi S.; Haque, Mohammad R.; Thurston, David E.; Zinzalla, Giovanna
Synthesis, 2011 , # 14 art. no. N24311SS, p. 2321 - 2333
反应条件
sodium periodate T=20°C; 2 h;
参考文献
Aboul-Fadl, Tarek; Rajeev, Gopalan; Broom, Arthur D.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 2 p. 445 - 451
反应条件
diisobutylaluminium hydride procedure of Fujii;
参考文献
Kelly, T. Ross; Lebedev, Rimma L.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2197 - 2205
反应条件
ozone; acetic acid; zinc 1.) methylene dichloride, methanol, -78 deg C, 2.) overnight; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 15 p. 3457 - 3465
反应条件
1: With dimethyl sulfoxide in dichloromethane T=-78°C; 1 h; 2: With triethylamine in dichloromethane T=-78 - 20°C;
参考文献
US2005/165089 A1, ;
Page/Page column 35 ;
反应条件
1: tetrahydrofuran 2: 87 percent / bleach; KHCO3; KBr / poly(vinyl alcohol)-graft-poly(ethylene glycol) TEMPO resin / CH2Cl2 / 0.5 h / 20 °C / pH 9.1 View Scheme
参考文献
Chemical Communications, , # 21 p. 2136 - 2138
反应条件
hydrogenchloride; sodium hydroxide in water; ethyl acetate
反应条件
hydrogenchloride; sodium hydroxide in water; ethyl acetate
参考文献
Norden, Benget; Wittung, Pernilla; Buchardt, Ole; Egholm, Michael; Nielsen, Peter E.; Berg, Rolf
Patent: US6228982 B1, 2001 ;
反应条件
hydrogenchloride; sodium hydroxide in water; ethyl acetate
参考文献
Buchardt, Ole; Egholm, Michael; Nielsen, Peter Eigil; Berg, Rolf Henrik
Patent: US6713602 B1, 2004 ;
