6,7-二羟基-4-甲氧基异黄酮合成路线 (共 6 条)
反应条件
boron trifluoride diethyl etherate; methanesulfonyl chloride
T=100°C; 2 h;
参考文献
Vasquez-Martinez, Yesseny; Ohri, Rachana V.; Kenyon, Victor; Holman, Theodore R.; Sepulveda-Boza, Silvia
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 23 p. 7408 - 7425
反应条件
boron trifluoride diethyl etherate; acetic anhydride in diethyl ether; acetic acid
Heating;
参考文献
Jah, Hem Chandra; Zilliken, Fritz; Breitmaier, Eberhard
Angewandte Chemie, 1981 , vol. 93, # 1 p. 129 - 130
反应条件
recombinant human cytochrome P450 1A1 in phosphate buffer
T=37°C; pH=7.4; Enzyme kineticsProduct distribution; Further Variations:Reagents;
参考文献
Roberts, Dean W.; Doerge, Daniel R.; Churchwell, Mona I.; Da Costa, Goncalo Gamboa; Marques, M. Matilde; Tolleson, William H.
Journal of Agricultural and Food Chemistry, 2004 , vol. 52, # 21 p. 6623 - 6632
反应条件
hydrogen; palladium on activated charcoal in 1,4-dioxane; ethanol
T=20°C; 6 h;
参考文献
Vasquez-Martinez, Yesseny; Ohri, Rachana V.; Kenyon, Victor; Holman, Theodore R.; Sepulveda-Boza, Silvia
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 23 p. 7408 - 7425
反应条件
sulfuric acid; hydrogen; acetic acid; palladium on activated charcoal
T=20°C; 14 h;
参考文献
Vasquez-Martinez, Yesseny; Ohri, Rachana V.; Kenyon, Victor; Holman, Theodore R.; Sepulveda-Boza, Silvia
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 23 p. 7408 - 7425
反应条件
O-methyl transferase from cell-free extract of Citrus mitis; [methyl-14C]-S-adenosyl-L-methionine; 2-hydroxyethanethiol in water; dimethyl sulfoxide
T=35°C; 0.5 h; pH 7.5 buffer; Product distribution;
参考文献
Brunet, Gunter; Ibrahim, Ragai K.
Phytochemistry (Elsevier), 1980 , vol. 19, p. 741 - 746