雄甾-1,4-二烯-3,17-二酮合成路线 （共 75 条）
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in o-di-fluorobenzene; dimethyl sulfoxide T=85°C; 48 h;
参考文献
Nicolaou; Zhong; Baran
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7596 - 7597
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in o-di-fluorobenzene; dimethyl sulfoxide T=70°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 10 p. 2245 - 2258
反应条件
PhIO2; benzeneseleninic anhydride in benzene 12 h; Heating;
参考文献
Barton, Derek H. R.; Godfrey, Christopher R. A.; Morzycki, Jacek W.; Motherwell, William B.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1947 - 1952
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane 8 h; Ambient temperature;
参考文献
Alper, Howard; Kwiatkowska, Caroline; Petrignani, Jean-Francois; Sibtain, Fazle
Tetrahedron Letters, 1986 , vol. 27, # 45 p. 5449 - 5450
反应条件
Mycobacterium neoaurum VKPM Ac-1656; styrene-divinylbenzene copolymer; soybean meal; ammonium phosphate monobasic; urea in water T=30°C; pH=6.8 - 7.2;
参考文献
Russian Journal of Bioorganic Chemistry, , vol. 33, # 3 p. 354 - 358
反应条件
unidentified fungal species isolated from grinded corn in water T=37°C; pH=7; 1 h; aq. phosphate bufferMicrobiological reactionEnzymatic reaction;
参考文献
Journal of Steroid Biochemistry and Molecular Biology, , vol. 119, # 3-5 p. 161 - 170
反应条件
tert-butyldimethylsilyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane T=0 - 20°C;
参考文献
Steroids, , vol. 75, # 7 p. 513 - 516
反应条件
toluene-4-sulfonic acid in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Steroids, , vol. 72, # 1 p. 60 - 63
反应条件
8-hydroxy-quinoline in water; N,N-dimethyl-formamide 72 h; Myc. mucosum 3-AP;
参考文献
Pharmaceutical Chemistry Journal, , vol. 16, # 6 p. 478 - 483
Khimiko-Farmatsevticheskii Zhurnal, , vol. 16, # 6 p. 722 - 727
反应条件
1: unidentified fungal species isolated from grinded corn / water / 1 h / 37 °C / pH 7 / aq. phosphate buffer; Microbiological reaction; Enzymatic reaction 2: unidentified fungal species isolated from grinded corn / water / 1 h / 37 °C / pH 7 / aq. phosphate buffer; Microbiological reaction; Enzymatic reaction View Scheme
参考文献
Journal of Steroid Biochemistry and Molecular Biology, , vol. 119, # 3-5 p. 161 - 170
