potassium hydride in diethylene glycol dimethyl ether
T=90°C; 2 h;
参考文献
Cohen, Theodore; Sherbine, James P.; Matz, James R.; Hutchins, Robert R.; McHenry, Barry M.; Willey, Paul R.
Journal of the American Chemical Society, 1984 , vol. 106, # 11 p. 3245 - 3252
1: 1-bromo-2-methyl-1-propene With magnesium in tetrahydrofuran
2: 1-bromocyclohexane With N,N,N',N,-tetramethylethylenediamine; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 1.5 h; Further stages.;
参考文献
Cahiez, Gerard; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2007 , vol. 9, # 17 p. 3253 - 3254
1: 1-bromo-2-methyl-1-propene With magnesium in tetrahydrofuran
2: 1-trans-IODO-4-CYCLOHEXYL With N,N,N',N,-tetramethylethylenediamine; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 1.5 h; Further stages.;
参考文献
Cahiez, Gerard; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2007 , vol. 9, # 17 p. 3253 - 3254
1: 1-bromo-2-methyl-1-propene With magnesium in tetrahydrofuran
2: cyclohexyl monochloride With N,N,N',N,-tetramethylethylenediamine; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 1.5 h; Further stages.;
参考文献
Cahiez, Gerard; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2007 , vol. 9, # 17 p. 3253 - 3254
in dimethyl sulfoxide
T=35 - 40°C; 12 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
Me2CCHI in dimethyl sulfoxide
Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 12h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by GLC;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
