(R)-2-乙酰胺基-4-硝基苯丙氨酸合成路线 （共 7 条）
反应条件
hydrogen; lt;Rh(1(R),5(R),6(R)-1,6-bis(diphenylphosphinoxy)spirolt;4.4gt;nonanegt;+ in methanol T=25°C; P=760 Torr; 0.166667 h;
参考文献
Journal of the American Chemical Society, , vol. 119, # 40 p. 9570 - 9571
反应条件
hydrogen; Rh[(R)-H8-BDPAB(COD)]BF4 in ethanol T=20°C; P=1551.44 Torr; 0.166667 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 12, # 16 p. 2337 - 2342
反应条件
lipase AS 'Amano' T=35°C; pH=6.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Tetrahedron: Asymmetry, , vol. 23, # 18-19 p. 1338 - 1342,5
反应条件
1: triethylamine / water; N,N-dimethyl-formamide / 20 °C 2: lipase AS 'Amano' / 24 h / 35 °C / pH 6.5 / |Enzymatic reaction View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 23, # 18-19 p. 1338 - 1342,5
反应条件
1: aqueous Na2CO3 / anschliessend Behandeln mit wss. HCl 2: Gewinnung ueber das Brucin-Salz View Scheme
参考文献
Journal of the Chemical Society, , p. 1229
Org. Synth. Isotopes, , p. 303
反应条件
1: acetic acid anhydride; HNO3; NO2 2: aqueous Na2CO3 / anschliessend Behandeln mit wss. HCl 3: Gewinnung ueber das Brucin-Salz View Scheme
参考文献
Journal of the Chemical Society, , p. 1229
Org. Synth. Isotopes, , p. 303
反应条件
Gewinnung ueber das Brucin-Salz;
参考文献
Journal of the Chemical Society, , p. 1229
Org. Synth. Isotopes, , p. 303
